The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 12, 2007

Filed:

Aug. 25, 2005
Applicants:

Pooran Chand, Birmingham, AL (US);

Yahya El-kattan, Hoover, AL (US);

Pravin L. Kotian, Hoover, AL (US);

Inventors:

Pooran Chand, Birmingham, AL (US);

Yahya El-Kattan, Hoover, AL (US);

Pravin L. Kotian, Hoover, AL (US);

Assignee:

BioCryst Pharmaceuticals, Inc., Birmingham, AL (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07D 207/06 (2006.01); C07D 207/08 (2006.01); C07D 207/09 (2006.01);
U.S. Cl.
CPC ...
Abstract

Two syntheses are provided; one for the preparation of (3R,4R)-4-(hydroxymethyl)pyrrolidin-3-ol, and other for the preparation of (3S,4R)-4-(hydroxymethyl)pyrrolidin-3-ol. (3R,4R)-4-(hydroxymethyl)pyrrolidin-3-ol is prepared using the achiral ylide prepared from benzylamine instead of phenethylamine (Scheme 3) which provides a crystalline intermediate. The synthesis of (3S,4R)-4-(hydroxymethyl)pyrrolidin-3-ol is achieved from (S)-diethylmalate as described in Scheme 4. A process for preparing camphor sultam is also provided.


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