The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 7193114 B1

PDF
Full Text
Expired
Date of Patent:
Mar. 20, 2007

Filed:

Jan. 14, 2004
Applicants:

Dean F. Martin, Tampa, FL (US);

Craig A. Bowe, Tampa, FL (US);

Inventors:

Dean F. Martin, Tampa, FL (US);

Craig A. Bowe, Tampa, FL (US);

Assignee:

University of South Florida, Tampa, FL (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 381/00 (2006.01); C07C 31/34 (2006.01);
U.S. Cl.
CPC ...
Abstract

The present invention attaches a molecule that contains a hydroxyl group (OH) attached to a carbon chain which is attached to a coordinating atom or atoms, the acidity of which is greater than that of silica (i.e., pKA <10). The condensation is achieved by mixing silica gel, appropriate amount of ligand, and a drop of conc. sulfuric acid in toluene in a flask attached to a Dean-Stark tube. Heating of the mixture is continued until the amount of water, obtained by azeotropic distillation and condensation, reaches a constant value. Toluene is filtered off, and recycled. The supported ligand is dried under reduced pressure to remove residual toluene. The composite (ligand attached to silica) can then be used by batch or column method to remove heavy metal ions from aqueous solution.


Find Patent Forward Citations

Martin, Dean. (2007). Extraction of metals by mercaptans attached to silica gel by azeotropic distillation (U.S. Patent No. 7193114). U.S. Patent and Trademark Office. https://idiyas.com/patent/badge/7193114

Data source: USPTO (United States Patent and Trademark Office) public patent records. Weekly synchronization. How IDiyas builds this profile

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