The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 26, 2006

Filed:

Aug. 23, 2002
Applicants:

Christopher John Harris, Worcester, GB;

Alan Craig Smith, Bedworth, GB;

Julie Ann Salter, Dudley, GB;

Inventors:

Christopher John Harris, Worcester, GB;

Alan Craig Smith, Bedworth, GB;

Julie Ann Salter, Dudley, GB;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07F 9/02 (2006.01);
U.S. Cl.
CPC ...
Abstract

A method for making β-ketophosphonates by reacting a trialkyl phosphonocarboxylate (such as triethyl phosphonoacetate) with an acyl halide (such as acetyl chloride) in a reaction involving ester formation, followed by decarboxylation, followed by purification. The reaction is run in a single solvent, which is not removed from the reaction mixture until the purification stage. Suitable solvents for this purpose include halogenated aromatic hydrocarbons (such as mono-chlorobenzene).


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