The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 7019037 B1

PDF
Full Text
Expired
Date of Patent:
Mar. 28, 2006

Filed:

Oct. 26, 2001
Applicants:

Thomas Samuel Zemanian, Richland, WA (US);

Glen Fryxell, Kennwick, WA (US);

Oleksiy A. Ustyugov, Spokane, WA (US);

Inventors:

Thomas Samuel Zemanian, Richland, WA (US);

Glen Fryxell, Kennwick, WA (US);

Oleksiy A. Ustyugov, Spokane, WA (US);

Assignee:

Battelle Memorial Institute, Richland, WA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 33/159 (2006.01); C09K 3/00 (2006.01); B01J 13/00 (2006.01);
U.S. Cl.
CPC ...
Abstract

Aerogels having a monolayer coating are described. The aerogel and a monolayer forming precursor are provided in a supercritical fluid, whereupon the aerogel and the monolayer forming precursor are reacted in said supercritical fluid to form a covalent bond between the aerogel and the monolayer forming precursor. Suitable aerogels are ceramic oxides such as silica, alumina, aluminosilicate, and combinations thereof. Suitable monolayer forming precursors include alkyl silanes, chlorosilanes, boranes, chloroboranes, germanes, and combinations thereof. The method may also include providing a surface preparation agent such as water, or hydroetching an aerogel to enhance the coating of the monolayer.


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