The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 01, 2005

Filed:

Aug. 11, 2000
Applicants:

Bruno Ceccaroli, Kristiansand, NO;

Kenneth Friestad, Kristiansand, NO;

Inventors:

Bruno Ceccaroli, Kristiansand, NO;

Kenneth Friestad, Kristiansand, NO;

Assignee:

Elkem ASA, , NO;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B033/037 ;
U.S. Cl.
CPC ...
Abstract

The invention relates to a method for purification of metallurgical grade silicon where a calcium containing compound is added to molten silicon prior to or after the silicon is tapped from the furnace. The silicon is cast and solidified at a relatively high cooling rate and the solidified silicon is crushed and subjected to a purification process consisting of two leaching steps. In the first leaching step the silicon is treated with an aqueous solution of FeClor FeCland HCl which causes disintegration of the silicon, and in the second leaching step the silicon is treated with an aqueous solution of HF or HF/HNO. Calcium-containing compound is added to the molten silicon in an amount necessary to provide between 0.3 and 0.95% by weight of calcium in the molten silicon and the weight ratio between Al and Fe in the molten silicon is regulated to between 0.5 and 2.0 by addition of aluminum to the molten silicon.


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