The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 18, 2003

Filed:

Nov. 09, 2001
Applicant:
Inventors:

Keith Allen Welp, Macungie, PA (US);

Anthony Rocco Cartolano, Orefield, PA (US);

Frederick Carl Wilhelm, Zionsville, PA (US);

William Joseph Mazzafro, Schnecksviile, PA (US);

Assignee:

Air Products and Chemicals, Inc., Allentown, PA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ;
U.S. Cl.
CPC ...
C07C / ;
Abstract

The invention is a process to regenerate monolith catalytic reactors employed in the liquid phase hydrogenation reactions, particularly those kinds of reactions involving nitroaromatic compounds. The catalytic metals in the monolith catalytic reactor are deactivated by carbonaceous and deactivating byproducts and must be regenerated to extend the catalyst service life and reduce costs. The regeneration process involves two steps: initially passing an oxidizing gaseous mixture through the monolith catalytic reactor at an elevated temperature and for a time sufficient to remove carbonaceous and deactivating byproducts; and then passing a reducing gas though the monolith catalytic reactor previously exposed to the oxidizing gas under conditions for reducing the catalytic metal to its reduced state.


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