The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 26, 2002

Filed:

Dec. 14, 1999
Applicant:
Inventors:

Peter Heitkämper, Dormagen, DE;

Klaus Jost, Dormagen, DE;

Stefan Penninger, Pulheim, DE;

Assignee:

Bayer Aktiengesellschaft, Leverkusen, DE;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C / ; C07C / ; C07C / ;
U.S. Cl.
CPC ...
C07C / ; C07C / ; C07C / ;
Abstract

Durene diisocyanate is prepared by reacting durene with nitric acid in sulfuric acid, catalytic hydrogenation of the dinitrodurene that is formed, and phosgenation of the resultant durene diamine in a conventional manner. The intermediate products dinitrodurene and durene diamine do not have to be worked up in a complicated manner as solid products, but can be worked up in dissolved form. The intermediate products dinitrodurene and durene diamine do not have to be isolated and purified in a complicated manner. but can be processed directly after preparation. Another advantage of this process is that only a single organic solvent need be used for the overall preparation process. Separation and re-use of spent acid in the conversion of durene with nitric acid also renders the process of the present invention significantly less environmentally harmful than the known processes of the prior art.


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