The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 10, 2002

Filed:

Aug. 20, 2001
Applicant:
Inventors:

Mahmoud F. Abdel-Rahman, Newark, DE (US);

Andrew M. Warchol, Wilmington, DE (US);

James W. Baker, Elkton, MD (US);

Assignee:

Agilent Technologies, Inc., Palo Alto, CA (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
G01N 2/762 ;
U.S. Cl.
CPC ...
G01N 2/762 ;
Abstract

An apparatus for and method of making a discharge ionization detector. The apparatus comprises a detector body, a detector cavity, located in the detector body and having a discharge electrode and an second discharge electrode, wherein an electric discharge runs between the second discharge electrode and the discharge electrode, and a signal electrode which attracts ionized molecules, an inlet interface, through which a discharge gas enters the detector, an analyte inlet, through which the analyte enters the detector cavity, and an outlet through which the analyte and discharge gas exit the detector body, wherein the apparatus is hermetically sealed. The apparatus is hermetically sealed by vacuum brazing the components to the detector body. The present invention can also have a detector volume as small as 10 micro-liters or less. The method comprises machining a body material to form a detector body, by forming a detector cavity, a column bore and a plurality of electrode bores, preparing the body surface for bonding, and bonding a plurality of electrodes, an inlet interface, a column interface and a vent interface to the detector body, whereby a hermetically sealed system is formed that has a detection zone volume of approximately 5-100 micro-liters.


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