The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 20, 2001

Filed:

Jul. 22, 1999
Applicant:
Inventors:

Jean-Florent Campion, Bois Colombes, FR;

Jean-Philippe Francois, Thones, FR;

Christelle Lavallade, Courdimanche, FR;

Philippe Oskeritsian, Rueil Malmaison, FR;

Jean-Maxime Saugrain, Le Vesinet, FR;

Assignee:

Alcatel, Paris, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B05D 7/00 ;
U.S. Cl.
CPC ...
B05D 7/00 ;
Abstract

Silica granules made up of mutually agglomerated silica soot particles are treated by placing the granules in a crucible inside a furnace which contains an inert gas mixed with a chlorine-containing compound and in which the temperature lies in the range 1000° C. to 1500° C. According to the invention, a crucible is used that is made of porous graphite firstly to increase the surface area of the crucible through which the chlorine-containing compound diffuses. This gives rise to faster exchange between the granules and the gas for given partial pressure of the chlorine-containing compound, thereby improving purification. Secondly, the difference between the chemical natures of the silicas and the crucible make the two materials inert relative to each other so that the granules do not adhere to the walls of the crucible, thereby making it possible to recover the granules without having to apply any mechanical operation that might contaminate them.


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