The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 16, 2001

Filed:

Nov. 17, 1999
Applicant:
Inventors:

Tao Wang, Corpus Christi, TX (US);

Jerry A. Broussard, Corpus Christi, TX (US);

H. Robert Gerberich, Corpus Christi, TX (US);

Assignee:
Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
B01J 2/358 ; B01J 2/340 ; B01J 2/342 ; B01J 2/356 ; B01J 2/344 ;
U.S. Cl.
CPC ...
B01J 2/358 ; B01J 2/340 ; B01J 2/342 ; B01J 2/356 ; B01J 2/344 ;
Abstract

A catalyst effective for the production of vinyl acetate by reaction of ethylene, oxygen and acetic acid, comprising a porous support on the porous surfaces of which is deposited catalytically effective amounts of metallic palladium and gold, and prepared by steps comprising impregnating the support with one or more aqueous solutions of water-soluble compounds of the metals, fixing the metals on the support as water-insoluble compounds in one or more fixing steps by reaction with an appropriate alkaline compound, and reducing the water-insoluble compounds of the catalytically active metals to their free metallic form in one or more reducing steps, at least one of the said reducing steps being carried out in an aqueous medium containing a reducing agent dissolved therein or through which a gaseous reducing agent is bubbled, and in which the support containing the fixed water-insoluble metal compounds is immersed, while sonicating, i.e., applying ultrasound waves to, such aqueous medium.


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