The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 28, 2001

Filed:

Jun. 14, 1999
Applicant:
Inventors:

Vesselin Manev, Gastonia, NC (US);

Walter Ebner, Gastonia, NC (US);

William Thompson, Gastonia, NC (US);

Stephen Dow, Gastonia, NC (US);

Assignee:

FMC Corporation, Philadelphia, PA (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C01G 4/512 ; C01G 4/502 ; C01G 4/700 ; C01G 5/700 ; H01M 4/50 ;
U.S. Cl.
CPC ...
C01G 4/512 ; C01G 4/502 ; C01G 4/700 ; C01G 5/700 ; H01M 4/50 ;
Abstract

A method of preparing a highly homogenous spinel Li,Mn,O,intercalation compound having a predetermined mean particle size and particle size distribution for 4 V secondary lithium and lithium ion cells is provided. The method comprises mixing at least one manganese compound having a predetermined particle size distribution with at least one lithium compound wherein the manganese compound has a mean particle size of between about 1 and 15 microns and the mean particle size of the lithium compound is less than that of the manganese compound The mixture is then fired in one or more firing steps within specific temperature ranges to form the Li,Mn,O,intercalation compound. Preferably, at least one firing step is at a temperature of between about 700° C. and 900° C. The Li,Mn,O,intercalation compounds may be used in the positive electrodes of secondary lithium and lithium ion cells to provide cells having high specific capacity, cycleability, and charge-discharge rate capability.


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