The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 26, 2001

Filed:

Aug. 06, 1999
Applicant:
Inventors:

Manfred Schmidt, Geinhausen, DE;

Christoph Klatte, Gründau, DE;

Kurt Kunz, Birstain, DE;

Josef Leutner, Grossheubach, DE;

Jürgen Ohlemacher, Maintal, DE;

Hans Peter Krimmer, Dietzenbach, DE;

Assignee:

Degussa-Huls AG, Frankfurt am Main, DE;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07D / ;
U.S. Cl.
CPC ...
C07D / ;
Abstract

A method for producing alkali metal salts or alkaline earth metal salts of 2,4-dicloro-6-hydroxy-s-triazine, especially the sodium salt, by reacting cyanuric chloride with an alkali hydroxide or alkaline earth hydroxide. 1 to 2.5 Equivalents of alkali hydroxide or alkaline earth hydroxide per mole cyanuric chloride in the form of an aqueous solution or suspension are placed in a receiver and cyanuric chloride in powder form or in the form of an aqueous suspension is added while maintaining a pH in the range of 9.5 to 14 and cooling. If less than a stoichiometric amount is added to the receiver, the remaining amount of alkali hydroxide or alkaline earth hydroxide is added during and/or after the addition of cyanide chloride, while maintaining the pH. The method can be carried out on an industrial scale and formation of the salt of monochlorodihydroxytriazine is largely avoided.


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