The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Feb. 13, 2001
Filed:
Feb. 19, 1999
Frédéric Amiche, Aulnay-Sous-Bois, FR;
Adrien Dromard, Lyons, FR;
Rhodia Chimie, Courbevoie Cedex, FR;
Abstract
The invention discloses an abrasive precipitation silica useable in toothpaste compositions, said silica having a BET specific surface ranging from 15 to 300 m,/g, a DOP oil absorption ranging from 40 to 160 ml/g, a median particle diameter of at least 10 &mgr;m, generally ranging from 12 to 30 &mgr;m, a particle cohesion factor of at least 85% about for a median particle diameter ranging from 12 to 20 &mgr;m. Method for preparing silica by reacting an alkaline metal silicate with an acidifying agent, to form a silica slurry, separating and optionally drying the recuperated silica suspension, the operation for forming the slurry being effected according to the following steps: a first step consisting in using one initial heel solution constituted of water, an electrolyte salt of the alkaline or alkaline-earth metal group and optionally of one acidobasic agent; a second step consisting in introducing the silicate and the acidifying agent, the reaction medium pH remaining constant from 4 to 7 and particularly from 5.8 to 6.7; and a third optional step, consisting in acidifying the reaction medium until a silica slurry with a pH of less than 6 and particularly of 4 is obtained. The silica is useful in toothpaste compositions. Toothpaste compositions containing the said silica are also disclosed.