The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 07, 2000

Filed:

Apr. 29, 1998
Applicant:
Inventors:

Niomi L Krzystowczyk, Orangeburg, SC (US);

Steven P Diefenbach, Baton Rouge, LA (US);

Edward A Burt, Lexington, SC (US);

Assignee:

Albemarle Corporation, Richmond, VA (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
B01J / ; B01J / ; B01J / ; C08F / ; C08F / ;
U.S. Cl.
CPC ...
502107 ; 502104 ; 502103 ; 502117 ; 502152 ; 502-5 ; 502522 ; 556187 ; 556182 ; 556179 ; 556175 ;
Abstract

A process is described which comprises heating a methylalumoxane solution in an aromatic hydrocarbon solvent at a temperature of at least 35.degree. C. for at least 0.5 hour in an inert, dry atmosphere such that the resulting heat-treated composition provides, in a supported metallocene catalyst produced using the heat-treated composition, increased activity as compared to the same supported metallocene catalyst produced in the same way except for using a portion of the methylalumoxane solution that has not been heat-treated. Before the heating the methylalumoxane of the solution contains from about 5 to about 35 mole percent unreacted trimethylaluminum, and was formed by partial hydrolysis of trimethylaluminum with free water in an organic solvent.


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