The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 25, 2000

Filed:

May. 05, 1999
Applicant:
Inventors:

Scott Donald Barnicki, Kingsport, TN (US);

Robert Sterling Kline, Jefferson City, TN (US);

James Alan Kenning, Longview, TX (US);

Anthony Dominick Messina, Longview, TX (US);

Assignee:

Eastman Chemical Company, Kingsport, TN (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07D / ;
U.S. Cl.
CPC ...
549538 ;
Abstract

A process for recovering 3,4-epoxy-1-butene from a vapor phase catalytic oxidation reactor effluent where 1,3-butadiene is reacted with oxygen over a silver catalyst, the process includes the steps of contacting the reactor effluent with an absorbent in an absorber and vaporizing in the absorber an effective amount of a non-reactive coolant to cool the absorber to a temperature of less than about 40.degree. C. and a pressure of less than about 4 bar. Advantageously, the vaporization of the non-reactive coolant proximate to the absorber allows the absorber to be operated at lower temperatures and pressures than heretofore possible and provides a further advantage of allowing higher O.sub.2 concentrations in the feed to the epoxidation reactor.


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