The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 26, 1999

Filed:

Mar. 24, 1997
Applicant:
Inventors:

Anna K Chen, Rahway, NJ (US);

Ramesh Kakarla, East Brunswick, NJ (US);

Dashan Liu, East Brunswick, NJ (US);

Michael J Sofia, Lawrenceville, NJ (US);

Thomas C Zebovitz, Colonia, NJ (US);

Assignee:

Intercardia, Inc., Research Triangle, NC (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07J / ; C07G / ; C07G / ;
U.S. Cl.
CPC ...
536-5 ; 536 185 ; 536124 ;
Abstract

The present invention relates to a process for the preparation and manufacture of 3-amino-substituted glycosylated bile acid derivatives. Intermediates and related compounds are also disclosed. In particular, the present invention permits the conversion of cholic acid esters to the 3-amino-7,12-bis(glucosyl)cholic acid esters via an azide intermediate. Conditions for the purification and isolation of the desired product is also disclosed to provide an overall manufacturing process suitable for large-scale production.


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