The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 22, 1998

Filed:

Aug. 26, 1996
Applicant:
Inventors:

Rei-Yu Judy Hwan, Sugarland, TX (US);

Mark Elliott Taylor, Orange, TX (US);

John Frederick Knifton, Austin, TX (US);

Melvin Ernest Stockton, Georgetown, TX (US);

John Ronald Sanderson, Leander, TX (US);

Assignee:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ; C07C / ; C07C / ; B01D / ;
U.S. Cl.
CPC ...
568697 ; 203 29 ; 203 45 ; 203 46 ; 203 73 ; 568698 ; 568699 ;
Abstract

Methyl tertiary butyl ether is prepared from contaminated TBA by reactively distilling the contaminated TBA in a reactive distillation column to provide a lower boiling isobutylene fraction and a higher boiling aqueous TBA fraction, by distilling the higher boiling aqueous TBA fraction to provide a lower boiling TBA fraction, by charging the lower boiling isobutylene fraction, the lower boiling tertiary butyl alcohol fraction and methanol to an etherification reactor to form an etherification reaction product, by distilling the etherification reaction product to provide a lower boiling fraction containing isobutylene, methanol and methyl tertiary butyl ether by charging the lower boiling fraction to a finishing reactor to react the isobutylene and methanol contained therein to from additional MTBE and by recovering MTBE from the etherification reaction product and the isobutylene conversion product.


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