The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 28, 1998

Filed:

Dec. 06, 1996
Applicant:
Inventors:

Michael David Hamlin, Brockport, NY (US);

Richard Wayne Connelly, Rochester, NY (US);

Assignee:

Eastman Chemical Company, Kingsport, TN (US);

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07D / ;
U.S. Cl.
CPC ...
549407 ;
Abstract

Disclosed is a process for whereby d-alpha-tocopheryl succinate (TS) can be crystallized in a short period of time by subjecting a fluid TS at particular temperature to a particular rate of shear for a particular time in order to accomplish crystallization. Then, while maintaining the crystallized TS at a temperature less than its melting point, we withdraw the crystallized TS from the region of shear flow. In a preferred embodiment of our process, crystallization is enhanced by use of a particular elongational rate for a particular time.


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