The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 17, 1998

Filed:

Nov. 29, 1996
Applicant:
Inventors:

James J Baiel, Morris Plains, NJ (US);

Larry O Jones, Baton Rouge, LA (US);

Ralph D Gray, Jr, Morristown, NJ (US);

Magdiel Agosto, Baton Rouge, LA (US);

Assignee:

Exxon Chemical Patents Inc., Houston, TX (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07D / ;
U.S. Cl.
CPC ...
203 56 ; 203 51 ; 549250 ;
Abstract

A process for recovering phthalic anhydride as a liquid from a vapor phase oxidation product which comprises mixing the vapor phase oxidation product having a temperature of about 130.degree. C. or greater with a first stream comprising a solvent having a boiling point in the range between about 150.degree. to 350.degree. C. and a freezing point of less than 40.degree. C., and, optionally, at least one by-product selected from the group consisting of: maleic anhydride, citraconic anhydride, benzoic acid and phthalic anhydride, in a contacting means such that a substantial portion of the phthalic anhydride contained within the vapor phase oxidation product transfers from the vapor phase to a liquid phase and a substantial portion of the first stream which are more volatile than phthalic anhydride transfer from the liquid phase to the vapor phase and wherein a vapor-to-liquid weight ratio in the range between about 2 to 20 is exhibited within the contacting means, thereby forming a liquid phase phthalic anhydride product having a phthalic anhydride concentration in the range between about 50-100 wt. %., preferably 90-100 wt. %, without the formation of an intermediate solid phase.


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