The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 03, 1998

Filed:

Jun. 25, 1996
Applicant:
Inventors:

Andrew James Casale, New Tripoli, PA (US);

Richard Van Carr, Allentown, PA (US);

Assignee:

Air Products and Chemicals, Inc., Allentown, PA (US);

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C / ; B01D / ;
U.S. Cl.
CPC ...
564422 ; 564305 ; 203 12 ; 203 13 ;
Abstract

This invention relates to an improved process for storing and transporting toluenediamine, particularly for long term storage or storage in large containers, e.g., shipboard containers. The improvement in the process resides in substantially reducing the melting or freezing point of anhydrous toluenediamine obtained by the fractional distillation of a reaction product generated by the hydrogenation of dinitrotoluene. Such melting point reduction is accomplished by maintaining a water concentration in the toluenediamine in an amount of from 5 to 15% by weight under molten conditions for storage and transport. Preferably the level of water maintained in the toluenediamine is from about 7 to 10% by weight.


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