The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 13, 1998

Filed:

Dec. 18, 1989
Applicant:
Inventors:

David Charles Deleeuw, Midland, MI (US);

Jonathan Lipowitz, Midland, MI (US);

Paul Pu-yuan Lu, Hacienda Heights, CA (US);

James Alan Rabe, Midland, MI (US);

Assignee:

Dow Corning Corporation, Midland, MI (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C01B / ; C04B / ;
U.S. Cl.
CPC ...
264 292 ; 264345 ; 419 17 ; 501 88 ; 423345 ; 423347 ;
Abstract

A process for the preparation of substantially polycrystalline silicon carbide fibers is provided. The fibers may be fabricated to have a small diameter and are thermally stable at high temperatures. The process is carried out by initially forming fibers from a preceramic polymeric precursor comprising methylpolysilane resins. The fibers are then infusibilized to render them nonmelting followed by a pyrolysis step in which the fibers are heated to a temperature in excess of 1600.degree. C. in a nonoxidizing atmosphere to form substantially polycrystalline silicon carbide fibers. The substantially polycrystalline silicon carbide fibers which are formed by the process of the present invention have at least 75% crystallinity and have a density of at least about 2.9 gm/cm.sup.3. The polymeric precursor or the fibers contain, or have incorporated therein, at least about 0.2% by weight boron. This incorporation of boron may be accomplished either prior to or during formation of the fibers or during at least one of the infusibilizing or pyrolyzing steps of the process.


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