The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 26, 1997

Filed:

Jun. 10, 1996
Applicant:
Inventors:

Jian Steven Qi, Buffalo, NY (US);

David E Albright, Niagara Falls, NY (US);

Garra C Lester, Eden, NY (US);

Assignee:

Other;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
G01N / ;
U.S. Cl.
CPC ...
436128 ; 436163 ; 436164 ;
Abstract

Disclosed is a method of determining whether a solvent contains a tautomeric cyclic 1,2-dione. It is first determined whether the pH of the solvent is acidic (<5), basic (>9), or neutral (5 to 9). If the pH is neutral, an acid or a base is added to make the pH acidic or basic, respectively. The UV absorbance at a first wavelength between about 230 nm and about 270 nm and at a second wavelength between about 280 and about 320 nm is determined. If the pH is acid, it is changed to basic and, if it is basic, it is changed to acidic. The UV absorbance at the first and second wavelengths is again determined. The presence of a tautomeric cyclic 1,2-dione is indicated if the absorbance at the first wavelength was greater when the solvent was acidic and the absorbance at the second wavelength was greater when the solvent was basic. The concentration of the tautomeric cyclic 1,2-dione can be determined by multiplying the change in absorbance by a constant.


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