The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Oct. 29, 1996
Filed:
Jan. 23, 1995
Applicant:
Inventors:
John Y Lee, Baton Rouge, LA (US);
Edward A Burt, Baton Rouge, LA (US);
Assignee:
Albemarle Corporation, Richmond, VA (US);
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07F / ; C07F / ; C07F / ;
U.S. Cl.
CPC ...
534 11 ; 556 43 ; 556 52 ; 556 53 ; 556 58 ; 556 70 ; 556 87 ; 556136 ; 556140 ; 556143 ;
Abstract
A process for making a metallocene, said process comprising the steps of (a) reacting an alkylsubstituted cyclopentadiene ligand, which contains a mixture of endo- and exo-isomers, with up to about a 10% excess over a stoichiometric amount of a deprotonation agent based on the amount of endo-isomers, so as to form a salt of said endo-isomers, (b) reacting the endo-isomer salt with a transition or actinide metal compound so as to form said metallocene and (c) optionally separating said exo-isomers and trace amounts of unreacted endo-isomers from said metallocene by distillation.