The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 03, 1995

Filed:

Sep. 16, 1993
Applicant:
Inventors:

Gerhard Keunecke, Pulheim, DE;

Adolf Arnold, Maintal, DE;

Sabine Butzke, Alzenau, DE;

Assignee:

Zimmer Aktiengesellschaft, Frankfurt, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C08B / ;
U.S. Cl.
CPC ...
536 30 ; 536 32 ; 536 38 ; 536 58 ;
Abstract

A process for the production of cellulose carbamate from cellulose and urea through the conversion of the cellulose with excess urea in an inert liquid organic reaction carrier at a temperature in the range of 130 .degree. to 160.degree. C., separation of the reaction carrier from the reaction mixture and washing of the reaction mixture with water. The cellulose is intimately mixed with an aqueous urea solution. Then the water in the solution is replaced with the organic reaction carrier, and the reaction of urea and cellulose is carried out in the presence of an inert gaseous carrier to remove the by-product ammonia. Thereafter, the organic reaction carrier remaining in the reaction product is replaced with an aqueous urea solution and the resulting suspension of cellulose carbamate in the urea solution is filtered and washed free of urea with water. No liquid ammonia is required in this process.


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