The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 04, 1994

Filed:

Mar. 30, 1993
Applicant:
Inventors:

Thomas C Herzberg, Afton Township, Washington County, MN (US);

Robert B Fletcher, St. Paul, MN (US);

Randall F Henderson, Cottage Grove, MN (US);

Assignee:
Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07D / ; C07C / ; C07C / ; C07C / ;
U.S. Cl.
CPC ...
544178 ; 544106 ; 549511 ; 564497 ; 564498 ; 564510 ; 564-2 ; 568580 ; 568581 ; 568682 ; 568 19 ; 568 24 ; 568 65 ; 570118 ; 570134 ; 570177 ;
Abstract

A process for the purification of a perfluorochemical composition comprises continuously mixing the perfluorochemical composition, comprising a liquid mixture of inert perfluorochemicals (e.g., perfluoroalkanes, perfluoroethers, perfluoroaminoethers, or perfluoroalkyl tertiary amines) and isomeric fluorohydrochemicals, with a stabilization composition comprising water-miscible alkanol and an aqueous solution of base (such as potassium hydroxide) made by dissolving the base in an amount of water sufficient to dissolve or disperse the fluoride salt by-products of the subsequent reaction of the base with the fluorohydrochemicals to form fluoroolefins, the amount of the alkanol in the stabilization composition being in stoichiometric excess of the amount needed to completely convert the fluoroolefins to alkoxyvinyl ethers. The process can be utilized to purify the product mixtures resulting from fluorination methods such as direct fluorination or ECF.


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Herzberg, Thomas. (1994). Continuous process for purifying perfluorochemical compositions (U.S. Patent No. 5352785). U.S. Patent and Trademark Office. https://idiyas.com/patent/badge/5352785

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