The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 20, 1994

Filed:

Nov. 12, 1992
Applicant:
Inventors:

Annick Pucci, Croissy sur Seine, FR;

Paul Mikitenko, Noisy le Roi, FR;

Massimo Zuliani, Rueil Malmaison, FR;

Assignee:

Institut Francais du Petrole, Rueil Malmaison, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D / ;
U.S. Cl.
CPC ...
203 14 ; 203 19 ; 203 46 ; 203 63 ; 203 75 ; 203 76 ; 203 77 ; 203 78 ; 203 79 ; 203 80 ; 203 99 ; 203D / ; 203D / ; 203D / ; 568913 ; 568916 ; 568918 ;
Abstract

For separating ETBE and ethanol the following principal stages are employed: (1) Extraction of ethanol by water, the raffinate being ETBE saturated in water and the extract an ethanol/water mixture containing a small proportion of ETBE; (2) Concentration of the above mixture, the distillate being a mixture close to the ethanol/water azeotrope in composition and containing a very small proportion of ETBE; (3) Heteroazeotropic distillation of this distillate in two coupled columns with an overhead decanter, this distillation using ETBE as azeotroping agent; the residue of the first column being ethanol which is ca. 99% by mole and the residue of the second column being practically pure water, this water and the water recovered during the concentration stage being used as extraction solvent in stage (1). Stage (3) may be an ethanol dehydration unit using ETBE as dehydrating agent.


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