The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 02, 1994

Filed:

Dec. 09, 1992
Applicant:
Inventors:

Charles B Blake, Guilden Sutton, GB;

James M Forsyth, Withington, GB;

Ann S Liow, Halton Village, GB;

Stephen J Adams, Great Sankey, GB;

Ralph J Doy, Saltburn, GB;

Rowland J Brierley, Yarn, GB;

Jane A Roberts, Hoole, GB;

Brian Schofield, Atherton, GB;

Neil D Shilling, Northwich, GB;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ; C07C / ;
U.S. Cl.
CPC ...
570165 ; 570166 ; 570167 ; 570168 ; 570169 ; 570177 ;
Abstract

Water present in a hot gaseous product stream from a reactor system A,B (FIG. 1 ) containing hydrogen fluoride is separated from the stream in order to eliminate a potentially corrosive combination of water and HF. The water is removed by contacting the gaseous product stream with liquid HF in a distillation column so as to obtain a bottoms product containing liquid HF and water and a top product containing dry HF and the product to be recovered. The invention encompasses the separation process, a vessel for carrying out the process (FIGS. 2 to 4), a control system for the liquid HF supply to the distillation column (FIGS. 5 and 6) and a recovery system for recovering HF employed during operation of the reactor system in different regimes employing HF as a fluorination agent, as a diluent during catalyst regeneration and/or catalyst prefluorination (FIG. 7 ).


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