The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Jul. 19, 1994
Filed:
Dec. 28, 1992
William A May, Boulder, CO (US);
Amax Inc., Englewood, CO (US);
Abstract
Flowable molybdenum metal powder of controlled particle size distribution is produced by stage-wise reduction wherein, in a first stage, molybdenum trioxide feed is preferably introduced at depth in a fluid bed of molybdenum dioxide and is reduced in an atmosphere containing at least 50% hydrogen, by volume, at a temperature between 560.degree. and 620.degree. C. and the product molybdenum dioxide is then reduced to molybdenum metal in a second stage fluid bed at a temperature between 1025.degree. C. and 1075.degree. C. in an atmosphere containing at least 50% hydrogen employed in amount of at least 2.75 times stoichiometric while controlling the off-gas dewpoint to be at least 21.degree. C. and controlling the off-gas hydrogen:water vapor ratio so as not to exceed 24:1 and removing the product spheroidal molybdenum metal particles from the bottom of the bed to prevent collapse of the bed.