The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Mar. 02, 1993
Filed:
Jun. 17, 1991
Luc Parent, Quebec, CA;
Alcan International Limited, Montreal, CA;
Abstract
A process for producing unagglomerated single crystals of aluminum nitride of low oxygen content having a size of at least 10 microns suitable for the reinforcement of metal, ceramic and polymeric matrix composite materials, and especially metal matrix materials. The process involves producing a reaction mixture of alumina (or a precursor), carbon (or a precursor), and an alkali metal oxide (or precursor such as a carbonate) as a crystal growth promoter or catalyst. The alkali metal oxide is present in an amount required for the formation of crystals of the required size, preferably in the range of 10-60 microns. The reaction mixture is subjected to a preheating step under nitrogen at a temperature in the range of 1600.degree.-1700.degree. and is then subjected to a heating step under nitrogen at a temperature in the range of 1800.degree.-1950.degree. C. This two-stage heating process ensures that the resulting crystals are of low oxygen content and thus good thermal conductivity. Particularly desirable crystals are produced if electrostatic precipitator dust is used as a source of the alumina, if petroleum coke or calcined anthracite coal is used as a source of the carbon and if the reaction is carried out in the presence of a porosity enhancer for the reaction mass, especially short cellulose fibres. The particles produced by the invention are in the form of large single crystals for good matrix reinforcement and have low oxygen and carbon contents. The invention extends to the particles produced by the process and to matrix composites reinforced with the particles.