The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 26, 1991

Filed:

Oct. 05, 1990
Applicant:
Inventors:

Daniel D Lindley, Portland, TX (US);

Thomas A Curtis, Tega Cay, SC (US);

Timothy R Ryan, Corpus Christi, TX (US);

Edward M de la Garza, Corpus Christi, TX (US);

Charles B Hilton, Corpus Christi, TX (US);

Thomas M Kenesson, Corpus Christi, TX (US);

Assignee:

Hoechst Celanese Corporation, Somerville, NJ (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ;
U.S. Cl.
CPC ...
568319 ; 568324 ;
Abstract

A continuous process is provided for the production of 4'-isobutylacetophenone (4-IBAP) comprising feeding liquid hydrogen fluoride (HF) and an acetylating agent into an extractor-reactor to form a first, HF-rich phase containing the acetylating agent, feeding isobutylbenzene (IBB) to the extractor-reactor to form a second, IBB-rich phase which is contacted with said first, HF-rich phase in a manner such that the acetylating agent reacts with IBB to form 4-IBAP which is extracted into the first, HF-rich phase, and a light IBB-rich second phase containing the bulk of unreacted IBB, externally recycling said second, IBB-rich phase to the IBB feed point in combination with fresh IBB to make up for IBB consumed in the reaction and that and dissolved in the HF-rich phase, and withdrawing HF-rich phase containing 4-IBAP from the extractor-reactor.


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