The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 26, 1991

Filed:

Dec. 24, 1988
Applicant:
Inventors:

Jurgen Weber, Oberhausen, DE;

Detlef Kampmann, Bochum, DE;

Claus Kniep, Oberhausen, DE;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C / ;
U.S. Cl.
CPC ...
544-1 ; 544-2 ; 544-3 ; 544 59 ; 544 63 ; 544106 ; 544162 ; 544179 ; 544180 ; 544224 ; 546 26 ; 546143 ; 546159 ; 546244 ; 546264 ; 546304 ; 548122 ; 548123 ; 548124 ; 548125 ; 548130 ; 548138 ; 548161 ; 548190 ; 548212 ; 548222 ; 548233 ; 548244 ; 548245 ; 548251 ; 548255 ; 548256 ; 548257 ; 548379 ; 548337 ; 548351 ; 548372 ; 548483 ; 548557 ; 548951 ; 548953 ; 5482672 ; 549-9 ; 549 10 ; 549 11 ; 549 12 ; 549 21 ; 549 28 ; 549 38 ; 549 68 ; 549 88 ; 549225 ; 549243 ; 549253 ; 549321 ; 549346 ; 549371 ; 549394 ; 549404 ; 549439 ; 549467 ; 549480 ; 549505 ; 549510 ; 564308 ; 564309 ; 564374 ; 564381 ; 564382 ; 564391 ; 564398 ; 564446 ; 564462 ; 564473 ;
Abstract

A process for the preparation of tertiary N,N-dimethylamines by the reaction of primary amines, formaldehyde, and hydrogen under pressure and at elevated temperature in the presence of a nickel-containing hydrogenation catalyst in the liquid phase. The hydrogenation catalyst is suspended in a solvent, the nickel concentration is 0.1 to 10% by weight, based on the primary amine. The starting materials are separate from each other, brought to 80.degree. to 150.degree. C. and 1 to 15 MPa and fed into the catalyst suspension simultaneously with stirring and reacted in one step to form the tertiary N,N-dimethylamines.


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