The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 05, 1991

Filed:

Sep. 26, 1989
Applicant:
Inventors:

Larry Y Yen, Tewksbury, MA (US);

George Lopatin, Newton Centre, MA (US);

Howard Malarkey, Lowell, MA (US);

David Soane, Piedmont, CA (US);

Assignee:

Millipore Corporation, Bedford, MA (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C08L / ; B01D / ;
U.S. Cl.
CPC ...
264 41 ; 55 16 ; 21050022 ; 21050023 ; 21050036 ; 21050042 ; 26417717 ; 2641 / ; 2642091 ; 521 61 ; 521 64 ; 521134 ; 521145 ;
Abstract

Microporous or open ultrafiltration poly (tetrafluoroethylene-co-perfluoro-(alkyl vinyl ether)) (PFA) or poly (tetrafluoroethylene-co-hexafluoropropylene) (FEP) film membrane or hollow fibers having open pores are formed from a melt blend of 10 to 35 weight percent of the PFA or FEP and a chlorotrifluoroethylene oligomer solvent. The melt blend is shaped and one or more surfaces of the shaped melt blend are coated with the solvent prior to phase separation of the melt blend. Coating the membrane with solvent during shaping results in membrane having larger pores on that membrane surface as compared to membranes not coated with solvent. The shaped melt blend is cooled to effect phase separation and crystallization of the PFA or FEP from the blend. The solvent is separated from the PFA or FEP by extraction and the porous PFA or FEP is heat set under restraint to prevent shrinkage. In one embodiment of this invention the dry film membrane recovered after extraction or the membrane wet with extraction liquid is stretched in the cross-web direction to below its breaking limit, dried, restrained and then heat-set.


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