The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 16, 1990

Filed:

Dec. 21, 1989
Applicant:
Inventors:

Robert W Mason, Lake Charles, LA (US);

Thomas C Parker, Sulphur, LA (US);

Assignee:

Olin Corporation, Cheshire, CT (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07D / ;
U.S. Cl.
CPC ...
544192 ;
Abstract

A process for the purification of crude cyanuric acid containing aminotriazine compounds as impurities which comprises digesting the crude cyanuric acid in an aqueous solution containing low concentrations of a mineral acid. The mineral acid is, for example sulfuric acid, nitric acid, hydrochloric acid, or phosphoric acid. The digestion is operated at a temperature in the range of from about 120.degree. C. and about 220.degree. C. and autogenous pressure using a stoichiometric ratio of sulfuric acid to aminotriazine compounds of less than 1, to produce a slurry of purified cyanuric acid in an acid depleted ammonium sulfate solution. Purification of cyanuric acid by the process of the present invention permits a substantial reduction in the amounts of acid used in the digestion and the base required for ammonia stripping and neutralization of the spent acid from the digestion. This provides significant cost savings in the digestion and waste treatment methods.


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