The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
May. 29, 1990
Filed:
Mar. 08, 1989
Applicant:
Inventors:
Charles W Matthews, Orangeburg, SC (US);
Eric S Batman, Belleville, IL (US);
Jeffrey F King, Orangeburg, SC (US);
Assignee:
Ethyl Corporation, Richmond, VA (US);
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ; C07C / ;
U.S. Cl.
CPC ...
568756 ; 568749 ;
Abstract
Aluminum phenoxide catalyst is removed from a phenolic alkylation mixture by adding 15-30 moles of water per mole of aluminum phenoxide to the alkylation mixture and holding at about 30.degree.-100.degree. C. for 10-60 minutes to form solids and heating the wet mixture to 120.degree.-160.degree. C. and holding at that temperature until filterable particulates form. The particulates can be readily filtered to obtain a substantially aluminum-free filtrate.