The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Apr. 10, 1990
Filed:
Aug. 31, 1988
Keith Hall, Altrincham, GB;
Philip A Freedman, Hartford, GB;
Elizabeth J Jumeau, Leftwich, GB;
Roger Guilluy, St Bonnet de Mure, FR;
Christiane Pachiaudi, Meyrieu, FR;
Jean P Riou, Lyon, FR;
VG Instruments Group Limited, Crawley, GB;
Abstract
The invention provides a method and apparatus for the mass spectrometric determination of the isotopic composition of an element comprised in a sample by gas chromatography-isotopic ratio mass spectrometry. As a sample elutes from the column of the gas chromatograph it enters a sample conversion means which converts the element to an analysis gas (a gas comprising the element in elemental form or in the form of a simple compound, e.g. nitrogen or carbon dioxide) which is admitted into the mass spectrometer only during a second time interval corresponding to the elution of the peak containing the sample from the column. One or more calibration samples of a reference gas are admitted into the spectrometer during first time intervals which do not overlap the second time interval, thereby minimizing the contribution of the analysis gas to the reference gas mass analysis, and vice versa. Various devices are provided to minimize disturbance to the flow of gas into the spectrometer during practice of the method.