The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 10, 1989

Filed:

Apr. 04, 1986
Applicant:
Inventors:

Yuhshi Luh, Orange, CT (US);

Peter S Forgione, Stamford, CT (US);

Assignee:

American Cyanamid Company, Stamford, CT (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ;
U.S. Cl.
CPC ...
560345 ;
Abstract

Isophorone diisocyanate, 3-isocyanatomethyl-3,5,5-trimethylcyclohexylisocyanate (IPDI) is prepared by liquid phase thermolysis of the corresponding bis-carbamic acid ester into the corresponding isocyanate and alcohol, respectively, in the presence of a highly selective metal oxide catalyst (SnO.sub.2 and/or CuO). Typically, the cracking reaction is carried out at a temperature from 225.degree. to 350.degree. C., at a pressure of from 20 to 50 mm Hg. These catalysts give high IPDI yields with high conversions of the carbamic acid esters.


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