The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 03, 1989

Filed:

Nov. 30, 1987
Applicant:
Inventors:

Edgar Bilger, Hasselroth, DE;

Hubert Wolf, Hammersbach, DE;

Assignee:

Degussa Aktiengesellschaft, Frankfurt am Main, DE;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
G01N / ;
U.S. Cl.
CPC ...
436109 ; 422 88 ; 422 86 ; 422 91 ; 436164 ;
Abstract

According to the invention, cyanide concentrations of approximately 0.001 to 5 mg cyanide/1 are colorimetrically determined in a continuous manner by means of the known cyanidepicric acid color reaction. The solution containing free cyanide and/or cyanide releasable from cyanocomplexes is converted in a system enclosed in a gas-tight manner in the presence of chelate complexing agents, picric acid and alkaline buffer systems in 1-60 minutes at 50.degree.-120.degree. C. to the color complex and the absorbency is measured spectrophotometrically. The method avoids the extraction step which was previously necessary under 0.2 mg CN/1, avoids errors due to HCN gas evolution losses, is easy to manage, not prone to trouble and suitable for the continuous monitoring of waste-water streams or for controlling cyanide detoxification methods.


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