The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 13, 1989

Filed:

Jan. 15, 1988
Applicant:
Inventors:

Robert V Hess, Newport News, VA (US);

Billy T Upchurch, Virginia Beach, VA (US);

Kenneth G Brown, Virginia Beach, VA (US);

Irvin M Miller, Newport News, VA (US);

David R Schryer, Hampton, VA (US);

Barry D Sidney, Gloucester, VA (US);

George M Wood, Newport News, VA (US);

Ronald F Hoyt, Tabb, VA (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
B01J / ; B01J / ;
U.S. Cl.
CPC ...
502 53 ; 20415751 ; 372 59 ; 502 38 ; 502339 ; 502352 ;
Abstract

A method of exchanging rare-isotope oxygen for common-isotope oxygen in the top several layers of an oxide-containing catalyst is disclosed. A sample of an oxide-containing catalyst is exposed to a flowing stream of reducing gas in an inert carrier gas at a temperature suitable for the removal of the reactive common-isotope oxygen atoms from the surface layer or layers of the catalyst without damaging the catalyst structure. The reduction temperature must be higher than any at which the catalyst will subsequently operate. Sufficient reducing gas is used to allow removal of all of the reactive common-isotope oxygen atoms in the top several layers of the catalyst. The catalyst is then reoxidized with the desired rare-isotope oxygen in sufficient quantity to replace all of the common-isotope oxygen that was removed.


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