The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
May. 02, 1989
Filed:
Mar. 21, 1988
Applicant:
Inventors:
Bernd Makowka, Bergisch-Gladbach, DE;
Hans-Dieter Block, Leverkusen, DE;
Assignee:
Bayer Aktiengesellschaft, Leverkusen, DE;
Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C / ;
U.S. Cl.
CPC ...
560204 ; 560190 ;
Abstract
An improved process for the preparation of dimethylmaleate by the esterification of maleic acid anhydride, maleic acid monomethylester, maleic acid or mixtures thereof with methanol in the presence of catalytic quantities of sulphuric acid, which comprises carrying out the esterification reaction within 20 to 120 minutes in a multistage bubble cap column reactor at temperatures of from 90.degree. to 140.degree. C. and with methanol excesses of from 0.4 to 2.0 mole per mole of the dimethylmaleate to be produced.