The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 17, 1989

Filed:

Dec. 22, 1987
Applicant:
Inventors:

Lonnie G Hazlitt, Lake Jackson, TX (US);

Daniel G Moldovan, Danbury, TX (US);

Assignee:

The Dow Chemical Company, Midland, MI (US);

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
G01N / ;
U.S. Cl.
CPC ...
73 53 ; 73 6 / ;
Abstract

A method and apparatus for analyzing a solution of a crystalline or a semi-crystalline polymer sample to determine a crystallinity versus weight percent profile concurrently with viscosity average molecular weight. The polymer sample is first precipitated from solution over a cooling temperature gradient to produce a precipitated polymer sample, which is precipitated as a function of its crystallinity. The precipitated polymer sample is then eluted and redissolved over a heating temperature gradient to produce successive fractions of a fractionated polymer sample solution, which are measured to produce concentration and specific viscosity data from which the intrinsic viscosity and viscosity average molecular weight are calculated.


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