The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 05, 1988

Filed:

Jun. 02, 1987
Applicant:
Inventors:

Duane A Bude, St. Louis County, MO (US);

Ellen Y Lin, Chesterfield, MO (US);

Assignee:

Anheuser-Busch, Incorporated, St. Louis, MO (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C / ;
U.S. Cl.
CPC ...
560 68 ; 560 69 ;
Abstract

A process for recovering active gallotannin for reuse comprising the extracting of dried schoene sludge (about 5% moisture) with a mixture of about 88 vol. % acetone--12 vol. % water to solubilize the gallotannins. The solvent is evaporated off, the residue is treated with water to solublize the gallotannins. After filtration, the clarified water solution is extracted with ethyl acetate. Evaporation of ethyl acetate leaves purified gallotannin which can be redissolved in water and spray dried to produce reusable powder. A preliminary step of separating yeast from the gallotannin protein complex involves treating with 60% acetone/40% H.sub.2 O at room temperature before making the solution about 88:12 acetone:water.


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