The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 07, 1986

Filed:

Feb. 21, 1985
Applicant:
Inventors:

Ares N Theodore, Farmington Hills, MI (US);

Robert A Pett, Franklin, MI (US);

Assignee:

Ford Motor Company, Dearborn, MI (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C04B / ;
U.S. Cl.
CPC ...
264 63 ; 264150 ; 2642091 ; 2641761 ;
Abstract

This invention relates to an extrusion method of preparing tubular green bodies, in particular those having thin walled thickness, which after burnout and sintering have properties similar or better than those of tubular bodies produced by isostatic pressing and are suitable for use in the sodium/sulfur battery. The method comprises extruding a mixture of 40-60 volume percent of sinterable particulate solids consisting essentially of a particle size distribution of beta'-alumina precursor particulate comprising alpha-alumina and 60-40 volume percent organic sacrificial binder consisting essentially of a thermoplastic block copolymer, plasticizers comprising two oils and two waxes, stiffening thermoplastic polymers and processing aids. In the preferred embodiment, the composition of the particulate comprises 8.85 weight percent Na.sub.2 O, 0.75 weight percent Li.sub.2 O and 90.4 weight percent Al.sub.2 O.sub.3 and the temperature of the material is maintained between about 135.degree.-150.degree. C. during extrusion. The die used to extrude the mixture has a ratio of the length of the die to the wall thickness of the tubular green body extruded of greater than about 5:1. The tubular green body is extruded over a mandrel.


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