The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Oct. 08, 1985
Filed:
Oct. 30, 1984
Applicant:
Inventor:
Thomas Schmidt, Haan, DE;
Assignee:
Bayer Aktiengesellschaft, Leverkusen, DE;
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D / ;
U.S. Cl.
CPC ...
544182 ;
Abstract
In the preparation of amino-3-ethylthio-6-tert.-butyl-1,2,4-triazin-5-one (I) by reacting 4-amino-3-mercapto-6-tert.-butyl-1,2,4-triazin-5-one (II) with an ethylating agent in aqueous alkali solution, the improvement which comprises contacting the reaction mixture with at least 50 g of petroleum ether per mole of starting compound (II) at a temperature of about 40.degree.-60.degree. C. thereby forming two liquid phases, and cooling the mixture down to about room temperature, whereby substantially pure isomer-free end product of the formula (I) crystallizes out.