The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 01, 1983

Filed:

Jul. 02, 1981
Applicant:
Inventor:

Thomas Hutson, Jr, Bartlesville, OK (US);

Assignee:

Phillips Petroleum Company, Bartlesville, OK (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D / ; C07C / ;
U.S. Cl.
CPC ...
568697 ; 203-3 ; 203 41 ; 203 70 ; 203D / ; 568699 ;
Abstract

Butenes are added to the methanol-containing methyl-tertiary-butyl ether (MTBE) reactor effluent fractionation to effect recovery of substantially methanol-free MTBE bottoms product. Methanol analysis taken below the fractionator feed locus manipulates control of butenes addition. In an embodiment, the methanol-butenes-containing overhead stream from the fractionation is treated over activated alumina to adsorb methanol, yielding a methanol-free butenes feed for HF alkylation of isobutane. The used adsorbent can be regenerated using hot butenes product and/or MTBE reactor feed vapor with the recovered methanol being recycled to the MTBE reaction.


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