The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 19, 1982

Filed:

Jan. 25, 1980
Applicant:
Inventors:

Robert Cole, Dudley, GB;

James E Stephenson, Birmingham, GB;

Assignee:

Albright & Wilson Ltd., Oldbury, GB;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ; B05D / ; C09D / ; C09D / ;
U.S. Cl.
CPC ...
564 12 ; 106 1817 ; 106 1819 ; 252608 ; 4273933 ; 564 15 ;
Abstract

An improved process for manufacturing tetrakis (hydroxymethyl) phosphonium amide condensation product without the formation of a precipitate. Urea or thiourea is added to the tetrakis (hydroxymethyl) phosphonium salt having an anion formed from a dibasic or tribasic or polybasic acid. The said salt is in aqueous solution. The pH of the aqueous solution of said salt is adjusted to the range of 4-6.5 when the urea or thiourea is added to the salt. The proportion of said salt to said urea or thiourea is 1:0.05-0.5 (molar). The sulphuric acid salt is preferred. The process produces an improved aqueous product substantially free of insolubles.


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