The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Jan. 12, 1982
Filed:
Apr. 21, 1980
Samuel L Yates, Columbia, SC (US);
Charles J Cole, Columbia, SC (US);
Albert H Wiesner, Columbia, SC (US);
John W Wagner, Petersburg, VA (US);
Allied Corporation, Morris Township, Morris County, NJ (US);
Abstract
A two-stage hydrolysis process for polymerizing epsilon-caprolactam is disclosed comprising a first stage from a temperature of about 180.degree. C.-260.degree. C., a pressure of 20 to 150 psig, for a period of about 0.5 to 4 hours, then before equilibrium conditions are reached a second stage at a temperature of about 200.degree. C.-260.degree. C., a pressure of about 100-900 Torr for a period of about 2 to 15 hours, while continuously removing most of the water so that water is removed both during hydrolyzation and during the subsequent polycondensation, whereby the cyclic dimer content of the shaped polymer article is below 0.2 percent by weight.