The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.
The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.
Patent No.:
Date of Patent:
Apr. 22, 1980
Filed:
Jan. 22, 1979
Applicant:
Inventors:
Terry J Nestrick, Midland, MI (US);
Rudolph H Stehl, Midland, MI (US);
Assignee:
The Dow Chemical Company, Midland, MI (US);
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D / ; B01J / ;
U.S. Cl.
CPC ...
55 67 ; 55386 ; 252428 ; 2524 / ; 252430 ; 252441 ; 568750 ; 568758 ;
Abstract
Highly effective chromatographic column packings are prepared by reacting hydroxyl groups on a silica surface with SiCl.sub.4 and then reacting the chlorosilylated surface with a polyglycol or polymeric glycol ester in a slurry reaction. Residual chlorosilane groups on the reacted surface are neutralized by reaction with methanol or other lower alkanol. The resulting modified silica has a bonded, essentially monomolecular organic surface film which provides thermal stability, uniform efficiency, and rapid analysis when the material is used as a column packing in gas-liquid chromatography.