The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 11, 1979

Filed:

Apr. 24, 1978
Applicant:
Inventors:

Frank C Fowler, Kansas City, MO (US);

Don H Smith, Dallas, TX (US);

Assignee:

Atlas Powder Company, Dallas, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C / ; B01D / ;
U.S. Cl.
CPC ...
260467 ; 203 11 ; 203 91 ; 260705 ;
Abstract

A method for separating an aqueous solution which contains minor amounts of nitrated esters which are only slightly soluble in water is provided. Separation of the nitrated esters, which include ethylene glycol dinitrate and nitroglycerin, is effected by contacting the aqueous solution with an organic phase of ethylene glycol dinitrate for a period of time sufficient to allow extraction of the nitroglycerin in solution into the ethylene glycol dinitrate phase. The organic ethylene glycol dinitrate phase is then separated from the aqueous solution, and the latter is distilled at a temperature of from about 50 degrees F. to about 200 degrees F. at a lower than atmospheric pressure. Upon completion of the separation process water, which is substantially free of nitrated esters, is suitable for discharge and return to a natural environment.


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