The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 04, 1979

Filed:

Dec. 22, 1977
Applicant:
Inventors:

David P Higley, Katonah, NY (US);

Gary L Culp, Sissonville, WV (US);

John W Crandall, Charleston, WV (US);

Scott M Farquhar, Charleston, WV (US);

Assignee:

Union Carbide Corporation, New York, NY (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D / ;
U.S. Cl.
CPC ...
203 72 ; 203 78 ; 203 98 ; 203D / ; 203D / ; 202153 ; 2603402 ; 2606 / ;
Abstract

This invention is concerned with a continuous process for separating higher boiling, heat sensitive components from a liquid product stream. It involves a rapid evaporation of the desired product of the stream in an evaporator which minimizes residence time, such as a falling film evaporator, and feeding the vapors and the remainder of the stream to a separation column where the vaporized products rise in the column. Part of the vaporized products are removed after condensation and then recycled back to the column as a reflux. This reflux after contacting one or more trays is collected and recycled to the evaporator and mixed with the product feed being treated. The liquid remainder of the feed stream is collected at the bottom of the column. The bottom of the column can be kept at a temperature which minimizes any breakdown of the heat sensitive components present therein and, if desired, the bottoms in the column can be quickly withdrawn for treatment elsewhere or for recycling back to the process. A desirable embodiment is to recycle a portion of the residue at the bottom of the column back to the evaporator.


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