The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 28, 1979

Filed:

Apr. 16, 1973
Applicant:
Inventors:

Roger W Lange, Maplewood, MN (US);

Harold G Sowman, Maplewood, MN (US);

Assignee:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C04B / ; C08K / ; C09C / ;
U.S. Cl.
CPC ...
428328 ; 106 50 ; 106 48 ; 106 57 ; 106 733 ; 106 7333 ; 106300 ; 423610 ; 252310 ; 252317 ; 264 15 ; 2641 / ; 264204 ; 428404 ; 428407 ;
Abstract

Solid, shaped and fired refractory articles, such as fibers and microspheres, of titanium dioxide are made by shaping, gelling, and firing titania sols. Said fibers can be made by extruding in air a viscous aqueous titania sol, and heating and firing the resulting green fiber to remove water, decompose and volatilize undesired constituents, and form a refractory fiber of polycrystalline titanium dioxide, which is useful, for example, to form refractory fabrics or as reinforcement for composites. Said microspheres can be made by dispersing droplets of an aqueous titania sol in an organic dehydrating liquid, separating the resulting green microspheres from the dehydrating liquid, and heating and firing the green microspheres to form solid refractory microspheres of polycrystalline titanium dioxide, which are useful, for example, in reflective signs or traffic marking surfaces. Said fired fibers and microspheres are preferably transparent to visible light with the titanium dioxide content thereof in its anatase form.


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